Catwoman initiates a series of thefts that cause Commissioner Gordon to summon Batman and Robin. But the importance of the crimes go beyond the taking of the objects involved. The Dynamic Duo eventually find Catwoman's lair. But Robin is whisked away while Batman is given a choice between two doors. If he picks the right door, he'll find Catwoman. If he picks the wrong one, he'll face certain doom. The hero makes the wrong selection and is about to be attacked by a tiger.

Batman evades the attacking tiger thanks to his utility belt. First, he scales the wall. Then, he uses a sonic device "to split the tiger's skull," as narrator William Dozier informs us. The hero still has to free Robin, who is facing a separate death trap. Once that task is completed, the Dynamic Duo are back on Catwoman's trail. It turns out the feline villain is after the lost treasure of Captain Manx, which is in a remote spot outside of Gotham City.

Catwoman makes her return known with a string of robberies. Hoping to lure her into a trap, Batman plants a news blurb giving the whereabouts of a rare canary, but Catwoman is tipped off and arrives prepared. Batman and Robin follow a lead to Catwoman's hideout, the Pink Sandbox, but soon discover that this villain has been waiting for them.

Catwoman disguises herself as a wealthy recluse - Minerva Matthews - to exchange a quarter million dollars for two Stradivarius violins. Once the instruments are safely in her hands, the villain reveals her true identity and demands the cash back. But Catwoman is surprised to learn that her business partner - Zubin Zucchini - is also not who he appears to be.

Now in charge of the Gotham State Pen, Ma Parker and her jailhouse full of criminal cohorts use it as their base of operations. No one suspects jailed prisoners of the crimes, but a clue picked up by Batman and Robin may lead them right to Ma's whereabouts.

The Catwoman "steals" the voice of a television talk-show host in the middle of an interview with Bruce Wayne. She plants clues to suggest either the Joker, Riddler or Penguin may have committed the crime. In the meantime, she has fooled Commissioner Gordon into thinking she has gone straight. She makes her first mistake when she masquerades as Miss Klutz, a dance instructor visiting Wayne Manor. Allergic to dogwood, she sneezes and gives herself away. Her next target is to "steal" the voices of British singers Chad and Jeremy. Batman and Robin eventually track her to a dance studio, where a fight erupts. After it appears the Dynamic Duo has triumphed over Catwoman's forces, she drugs them. The heroes are placed inside a chamber where the sounds of water dripping will be magnified many, many times and drive them insane.

Batman and Robin escape Catwoman's trap by hitting the precise note needed to shatter the glass chamber in which they're prisoners. They quickly get on the trail of Catwoman. The feminine feline criminal eventually "steals" the voices of Chad and Jeremy, Commissioner Gordon and talk-show host Allen Stephens. She blackmails the British government, which faces the lost of revenue from the taxes on Chad and Jeremy's performances. Batman and Robin eventually capture Catwoman and her gang, but not before Batman and Catwoman express obvious affection for each other.

Catwoman and the Sandman have teamed up, and they're after the fortunes of J. Pauline Spaghetti, a rich insomniac. Catwoman pulls a publicity stunt, getting the Sandman (under the guise of "Dr. Somnambula") an invitation to Spaghetti's penthouse - and her financial records. Batman and Robin investigate the situation, but soon find themselves trapped by the criminals.

Though Batman escapes the Sandman's trap, Robin is left to wander in a deadly maze. A clue leads Batman to Catwoman's lair, where he informs her of Sandman's plans to elope with J. Pauline Spaghetti and keep her fortunes to himself. Enraged by the Sandman's trickery, Catwoman sets out after him. Batman, with the now-rescued Robin, also follows, and the group meet up at Spaghetti's old deserted pasta factory.

The Catwoman manages to drug Robin. The junior member of the Dynamic Duo is now the Catwoman's mindless slave. Batman is on the trail of the sultry villain, but he's hampered by the fact he can't harm his partner. Eventually, Batman is trapped by the Catwoman. He's in a giant trap and Robin is cutting the rope that will cause a giant mouse trap to snap on Batman. The Catwoman offers Batman a choice -- die by Robin's hand or agree to be subjected to the same drug.

Batman agrees to let the Catwoman drug him. But he appears to have a headache and the Catwoman permits him to take an aspirin. After the drug is administered, Batman appears to assist Catwoman on her crime wave. However, the police receive anonymous telephone calls that enable them to pick up members of Catwoman's gang, including the drugged Robin. Meanwhile, the Gotham City police try to trace the hot line to the Batcave. Batman is there with Catwoman. He uses a device that foils the trace. Eventually, Batman reveals he hadn't taken an aspirin but his universal drug antidote that prevented the drug from working. Catwoman tries to flee on top of a warehouse near the Gotham River. Batman is in pursuit and corners her. But, unwilling to go straight, she falls into the river. Has she lost her life, or just one of her nine lives?

Catwoman is released from prison, and claiming she wants to enrich her education, enrolls at Gotham City University. She dresses one of her own henchmen as the Caped Crusader in order to frame him for a robbery. With Batman in jail, she goes ahead with her plan for a mass sit-in at Chimes Square. Catwoman is more than surprised when Batman himself shows up at the event. However, his efforts to expose the villainess are futile, and she prepares to terminate him and Robin in front of the whole crowd.

Catwoman goes ahead with her scheme to steal several Batagonian Cat's Eye opals, but she has trouble finding someone to fence them since such rare stones would be easily spotted. With little recourse left, she decides to turn them in for the reward money. It seems like the perfect job for her acquaintance, Freddy the Fence. But when he notices that the gems are fakes, Catwoman realizes she has been tricked by Batman and vows to get revenge on the Caped Crusader once and for all.